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The challenges of missions to the Moon and Mars presents NASA with the need for more advanced life support systems, including better technologies for CO2 removal in spacecraft atmospheres and extravehicular mobility units (EMU). Amine-coated single wall carbon nanotubes (SWCNT) have been proposed as a potential solution because of their high surface area and thermal conductivity. Initial research demonstrated the need for functionalization of SWCNT to obtain optimal adherence of the amine to the SWCNT support phase [1]. Recent efforts focus on the development of new methods to chemically bond amines to SWCNT. Synthesis and characterization methods for these materials are discussed and some preliminary materials characterization data are presented. The CO2 adsorption capacity for several versions of SWCNT supported amine-based CO2 scrubber materials is also determined.

At present, Nickel Hydrogen batteries are tested at Marshall Space Flight Center (MSFC) in support of the Hubble Space Telescope (HST) program. In previous years, Nickel Cadmium batteries were tested at MSFC in support of HST. The Nickel Cadmium Battery Expert System-2 (NICBES-2) was employed on the HST six battery test bed to evaluate the performance of the HST Electrical Power System (EPS). With the beginning of testing of the nickel hydrogen six battery test bed, NICBES-2 had to be converted to NICkel Hydrogen Battery Expert System (NICHES). This paper describes the conversion of the NICBES-2 to the NICHES as well as future plans for NICHES.

One of the primary safety concerns for Space Station Freedom pressurized modules is fire. Some Freedom modules are unattended for long periods of time. In other cases, enclosed, pressurized volumes are not open to crew monitoring. As a result, a fire detection system is required to continuously monitor all modules for combustion. This paper briefly reviews the overall design for the Freedom fire detection system, and the design of the two basic types of detectors: smoke and flame. The smoke detectors monitor particulates in small open areas, stand-offs, end-cones, and racks. The flame detectors survey open areas for radiation at wavelengths and intensities characteristic of combustion. Responses from detectors are evaluated by Freedom's data management system to determine the presence of combustion and to recommend appropriate action.

A primary concern in creating a water reclamation system for long-duration manned space flight is the control of microbial contamination which can jeopardize water quality, compromise human health, and degrade constituent materials of the system. The microbial ecology facility in the Analytical and Physical Chemistry Branch of the Materials and Processes Laboratory at NASA's Marshall Space Flight Center (MSFC) is addressing this concern by means of experiments investigating the interaction of bacterial species in the development of a biofilm and their response to the introduction of additional species or to disinfection. Both static and recycling water systems are used. In static experiments, varied sequence and timing of species introduction in binary bacterial biofilms on 316L stainless steel elucidate the mechanisms involved in biofilm formation.

Life Sciences research on Space Station will utilize rats to study the effects of the microgravity environment on mammalian physiology and to develop countermeasures to those effects for the health and safety of the crew. The animals will produce metabolic water which must be reclaimed to minimize logistics support. The condensate from the Research Animal Holding Facility (RAHF) flown on Spacelab Life Sciences-2 (SLS-2) in October 1993 was used as an analog to determine the type and quantity of constituents which the Space Station (SS) water reclamation system will have to process. The most significant organics present in the condensate were 2-propanol, glycerol, ethylene glycol, 1,2-propanediol, acetic acid, acetone, total proteins, urea and caprolactam while the most significant inorganic was ammonia. Microbial isolates included Xanthomonas, Sphingobacterium, Pseudomonas, Penicillium, Aspergillus and Chrysosporium.

Reversible adsorption on zeolite molecular sieve material allows selective removal of carbon dioxide (CO2) from spacecraft air without the use of expendables. The four-bed molecular sieve (4BMS) CO2 removal subsystem chosen for use on space station is based on proven Skylab technology and provides continuous CO2 removal from the cabin atmosphere and concentration for further processing downstream or venting overboard. A 4BMS subsystem has also been chosen to remove CO2 from air in the Systems Integration Research Facility (SIRF) at NASA/Johnson Space Center (JSC). After installation in the SIRF in 1992, the subsystem underwent extensive testing in which cycle time, process air flow rate, and process air inlet CO2 composition were varied. In order to obtain performance data required for integration, the subsystem was operated under both nominal and off-nominal conditions. Results of this testing are presented.

A program is being performed to design, fabricate, and test a metal hydride sorption cryocooler system capable of supplying periodic refrigeration at 10 K. The system is intended to cool a focal plane array for a low-earth orbit satellite. The refrigeration is effected by sublimating solid hydrogen at 10 K. The solid hydrogen is produced in a batch process by cooling, solidifying, and subcooling liquid hydrogen formed at 30 K by a Joule-Thomson expansion. The spent hydrogen from the sublimation and Joule-Thomson expansion is absorbed by two metal hydride sorption bed assemblies.

Computer models are currently being developed by NASA and major aerospace companies to characterize regenerative life support waste water reclamation bioreactors. Detailed models increase understanding of complex processes within the bioreactors and predict performance capabilities over a wide range of operating parameters. Bench-top scale bioreactors are contributing to the development and validation of these models. The purpose of the detailed bioreactor model is to simulate the complex water purification processes as accurately as possible by minimizing the use of simplifying assumptions and empirical relationships. Fundamental equations of mass transport and microbial kinetics were implemented in a finite-difference model structure to maximize accuracy and adaptability to various bioreactor configurations. The model development is based upon concepts and data from the available literature and data from the bench top bioreactor investigations.

Bioreactor technology for waste water reclamation in a regenerative life support system (RLSS) is currently being developed by a team of NASA and major aerospace companies. To advance this technology, several activities are being performed concurrently; these include conducting small-scale studies and developing computer models. Small-scale studies are being performed to characterize and enhance the bioprocesses occurring within the bioreactor. New bioreactor configurations have been investigated which improved total organic carbon degradation as well as nitrification, the polishing step which converts nitrogenous wastes into forms that are easily removable from the water. Small-scale studies have also been performed using an activated sludge reactor demonstrating that TOC reduction and nitrification can occur in a single reactor. Computer models have been developed to guide the laboratory studies and to assist in full-scale system design.

A regenerable metal oxide CO2 absorber is being developed for future Extravehicular Mobility Unit (EMU) applications. It was designed to fit the existing shuttle EMU without modification of the interfaces. Absorption and regeneration tests were performed with subscale and full-size laboratory absorbers. Data is presented for open and closed loop absorber tests that evaluate the effects of residence time, mass velocity, and internal temperature on performance, with emphasis is on the full-size test unit. Regeneration testing quantified the effects of temperature and air flow rate on desorption rate, and of various absorber cooling modes. Its objective was to optimize conditions for minimum peak power and minimum total energy consumption.

The baseline Environmental Control and Life Support System (ECLSS) for the International Space Station (ISS) includes regenerative and non-regenerative technologies for Temperature and Humidity Control (THC), Atmosphere Control and Supply (ACS), Fire Detection and Suppression (FDS), Atmosphere Revitalization (AR), Water Recovery and Management (WRM), Waste Management (WM), and Vacuum System (VS). The U.S. Lab module will contain complete THC and ACS subsystems and an open loop AR including a Carbon Dioxide Removal Assembly (CDRA), Trace Contaminant Control Subassembly (TCCS), and a Major Constituent Analyzer (MCA). An Oxygen Generation Assembly (OGA) is added with the U. S. Hab module, along with the WRM and WM subsystems. The final baseline configuration is a closed water loop and partially closed atmosphere loop and represents the best available mature technologies.

Eight SUMMA passivated sampling canisters were shipped to the Russian Space Station Mir in February of 1995 to assess ambient trace contaminant concentrations. Prior to flight, the canisters were injected with isotope labeled surrogates and internal standards to measure potential negative impacts on measurement accuracy caused by the trip environmental conditions of launch and return. Three duplicate canister samples were collected in parallel with Russian sorbent samples to acquire data for comparative purposes. A total of 32 target and 13 non-target volatile compounds were detected in each of the samples analyzed. The concentrations of the compounds remained relatively consistent for the three sampling events, and all of the concentrations of detected contaminants were well below both US and Russian Spacecraft Maximum Allowable Concentrations (SMAC). Five different fluorocarbons were consistently detected at relatively high concentrations.

The Water Processor Assembly (WPA) for use on the International Space Station (ISS) includes various technologies for the treatment of waste water. These technologies include filtration, ion exchange, adsorption, catalytic oxidation, and iodination. The WPA hardware implementing portions of these technologies, including the Particulate Filter, Multifiltration Bed, Ion Exchange Bed, and Microbial Check Valve, was recently qualified for chemical performance at the Marshall Space Flight Center. Waste water representing the quality of that produced on the ISS was generated by test subjects and processed by the WPA. Water quality analysis and instrumentation data was acquired throughout the test to monitor hardware performance. This paper documents operation of the test and the assessment of the hardware performance.

A trade study conducted in 2001 selected a rotary disk separator as the best candidate to meet the requirements for an International Space Station (ISS) Carbon Dioxide Reduction Assembly (CRA). The selected technology must provide micro-gravity gas/liquid separation and pump the liquid from 69 kPa (10 psia) at the gas/liquid interface to 124 kPa (18 psia) at the wastewater bus storage tank. The rotary disk concept, which has pedigree in other systems currently being built for installation on the ISS, failed to achieve the required pumping head within the allotted power. The separator discussed in this paper is a new design that was tested to determine compliance with performance requirements in the CRA. The drum separator and pump (DSP) design is similar to the Oxygen Generator Assembly (OGA) Rotary Separator Accumulator (RSA) in that it has a rotating assembly inside a stationary housing driven by a integral internal motor[1].

Researchers at Luna Innovations Inc. and the National Aeronautic and Space Administration's Marshall Space Flight Center (NASA MSFC) are developing an integrated fiber-optic sensor system for real-time monitoring of chemical contaminants and whole-cell bacterial pathogens in water. The system integrates interferometric and evanescent-wave optical fiber-based sensing methodologies to provide versatile measurement capability for both micro- and nano-scale analytes. Sensors can be multiplexed in an array format and embedded in a totally self-contained laboratory card for use with an automated microfluidics platform.

An important aspect of air revitalization for life support in spacecraft is the removal of carbon dioxide from cabin air. Several types of carbon dioxide removal systems are in use or have been proposed for use in spacecraft life support systems. These systems rely on various removal techniques that employ different architectures and media for scrubbing CO2, such as permeable membranes, liquid amine, adsorbents, and absorbents. Sorbent systems have been used since the first manned missions. The current state of key technology is the existing International Space Station (ISS) Carbon Dioxide Removal Assembly (CDRA), a system that selectively removes carbon dioxide from the cabin atmosphere. The CDRA system was launched aboard UF-2 in February 2001 and resides in the U.S. Destiny Laboratory module. During the past four years, the CDRA system has experienced operational limitations.

A dual-membrane gas trap is currently used to remove gas bubbles from the Internal Thermal Control System (ITCS) coolant on board the International Space Station (ISS). The gas trap consists of concentric tube membrane pairs, comprised of outer hydrophilic tubes and inner hydrophobic fibers. Liquid coolant passes through the outer hydrophilic membrane, which traps the gas bubbles. The inner hydrophobic fiber allows the trapped gas bubbles to pass through and vent to the ambient atmosphere in the cabin. The gas trap was designed to last for the entire lifetime of the ISS, and therefore was not designed to be repaired. However, repair of these gas traps is now a necessity due to contamination from the on-orbit ITCS fluid and other sources on the ground as well as a limited supply of flight gas traps. This paper describes a novel repair technique that has been developed that will allow the refurbishment of contaminated gas traps and their return to flight use.

A dual-membrane gas trap is currently used to remove gas bubbles from the Internal Thermal Control System (ITCS) coolant on board the International Space Station. The gas trap consists of concentric tube membrane pairs, comprised of outer hydrophilic tubes and inner hydrophobic fibers. Liquid coolant passes through the outer hydrophilic membrane, which traps the gas bubbles. The inner hydrophobic fiber allows the trapped gas bubbles to pass through and vent to the ambient atmosphere in the cabin. The gas removal performance and operational lifetime of the gas trap have been affected by contamination in the ITCS coolant. However, the gas trap has performed flawlessly with regard to its purpose of preventing gas bubbles from causing depriming, overspeed, and shutdown of the ITCS pump. This paper discusses on-orbit events over the course of the last year related to the performance and functioning of the gas trap.

The current dual-membrane gas trap is designed to remove gas bubbles from the Internal Thermal Control System (ITCS) coolant on board the International Space Station (ISS). To date it has successfully served its purpose of preventing gas bubbles from causing depriming, overspeed, and shutdown of the ITCS pumps. However, contamination in the ITCS coolant has adversely affected the gas venting rate and lifetime of the gas trap, warranting a development effort for a next-generation gas trap. Previous testing has shown that a hydrophobic-only design is capable of performing even better than the current dual-membrane design for both steady-state gas removal and gas slug removal in clean deionized water. This paper presents results of testing to evaluate the effects of surfactant contamination on the steady-state performance of the hydrophobic-only design.

This paper presents and discusses the results of an integrated 4-Bed Molecular Sieve (4BMS), mechanical compressor, and Sabatier Engineering Development Unit (EDU) test. Testing was required to evaluate the integrated performance of these components of a closed loop atmosphere revitalization system together with a proposed compressor control algorithm. A theoretical model and numerical simulation had been used to develop the control algorithm; however, testing was necessary to verify the simulation results and further refine the model. Hardware testing of a fully integrated system also provided a better understanding of the practical inefficiencies and control issues, which are unavailable from a theoretical model.